4Y7V

Structural analysis of MurU

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	93.2
Detector technology	PIXEL
Collection date	2013-10-18
Detector	DECTRIS PILATUS 2M
Wavelength(s)	1.0
Spacegroup name	P 61 2 2
Unit cell lengths	72.350, 72.350, 162.480
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	49.615 - 1.800
R-factor	0.2169
Rwork	0.215
R-free	0.25370
RMSD bond length	0.007
RMSD bond angle	1.074
Data reduction software	XDS
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.850
High resolution limit [Å]	1.800	1.800
Number of reflections	24133
<I/σ(I)>	27.7	0.91
Completeness [%]	99.9	99.9
Redundancy	20

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6	293	(NH4)2SO4, MES