4Y0I

GABA-aminotransferase inactivated by conformationally-restricted inactivator

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-B
Synchrotron site	APS
Beamline	23-ID-B
Temperature [K]	100
Detector technology	CCD
Collection date	2014-07-22
Detector	RAYONIX MX-300
Wavelength(s)	0.99
Spacegroup name	P 1 21 1
Unit cell lengths	69.483, 226.755, 71.425
Unit cell angles	90.00, 108.79, 90.00

Refinement procedure

Resolution	36.044 - 1.662
R-factor	0.1734
Rwork	0.172
R-free	0.20440
RMSD bond length	0.007
RMSD bond angle	1.105
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall
Low resolution limit [Å]	49.680
High resolution limit [Å]	1.500
Number of reflections	271091
<I/σ(I)>	4.5
Completeness [%]	97.0
Redundancy	3.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		298	0.1 M ammonium acetate, o.1 M Bis-Tris (pH: 5.5), 17% w/v PEG 10,000