4XZV
Crystal Structure of SLMO1-TRIAP1 Complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-05-22 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.98000 |
| Spacegroup name | P 1 |
| Unit cell lengths | 79.620, 80.680, 98.020 |
| Unit cell angles | 87.25, 85.62, 89.92 |
Refinement procedure
| Resolution | 97.620 - 3.580 |
| R-factor | 0.27528 |
| Rwork | 0.273 |
| R-free | 0.30927 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4xzs |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.663 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 97.620 | 3.670 |
| High resolution limit [Å] | 3.580 | 3.580 |
| Rmerge | 0.544 | |
| Number of reflections | 28326 | |
| <I/σ(I)> | 11.6 | 2.7 |
| Completeness [%] | 98.9 | 97.5 |
| Redundancy | 3.5 | 3.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 100 mM sodium formate, 12% (w/v) PEG 3350 |
