4XXU
ModA - chromate bound
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-ID |
| Synchrotron site | APS |
| Beamline | 22-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-10-15 |
| Detector | RAYONIX MX-300 |
| Wavelength(s) | 0.97872 |
| Spacegroup name | P 31 |
| Unit cell lengths | 84.049, 84.049, 60.239 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 34.470 - 1.430 |
| R-factor | 0.161 |
| Rwork | 0.160 |
| R-free | 0.18000 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.090 |
| Refinement software | PHENIX ((PHENIX.REFINE: 1.8.2_1309)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 1.430 |
| Number of reflections | 86664 |
| <I/σ(I)> | 3.476 |
| Completeness [%] | 99.5 |
| Redundancy | 5.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 289.15 | 0.2 M potassium iodide, 20% w/v PEG 3,350 |
