Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE BL19 |
| Synchrotron site | ESRF |
| Beamline | BL19 |
| Temperature [K] | 277 |
| Detector technology | CCD |
| Collection date | 1996-04-15 |
| Detector | CUSTOM-MADE |
| Wavelength(s) | 0.905 |
| Spacegroup name | P 65 |
| Unit cell lengths | 84.890, 84.890, 169.000 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 36.760 - 2.400 |
| R-factor | 0.1521 |
| Rwork | 0.151 |
| R-free | 0.17300 |
| Structure solution method | MIR |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.090 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | DAREFI |
| Refinement software | BUSTER (2.11.6) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 2.500 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Rmerge | 0.670 | |
| Number of reflections | 25724 | |
| <I/σ(I)> | 14 | 1.5 |
| Completeness [%] | 95.5 | 72.1 |
| Redundancy | 5.9 | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 300 | 1.6-1.9M sodium formate, 0.1M sodium acetate |
