4XOV
Structure of rsGreen0.7 in the green-off-state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-09-11 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.8856 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 31.992, 61.308, 105.739 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.038 - 1.200 |
R-factor | 0.1439 |
Rwork | 0.143 |
R-free | 0.16830 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.349 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.5.6) |
Refinement software | PHENIX (1.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.040 | 1.240 |
High resolution limit [Å] | 1.200 | 1.200 |
Rmerge | 0.157 | 0.613 |
Number of reflections | 125686 | |
<I/σ(I)> | 4.9 | 1.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 3.8 | 3.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 289 | 0.15 M NaBr, 30% PEG 2000 MME |