4XE8
Bacillus thuringiensis ParM with ADP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13B1 |
Synchrotron site | NSRRC |
Beamline | BL13B1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-10-10 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.000 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 55.657, 73.032, 114.269 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.934 - 2.381 |
R-factor | 0.2243 |
Rwork | 0.218 |
R-free | 0.27500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.732 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.3.0) |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 20.000 | 20.000 | 2.420 |
High resolution limit [Å] | 2.380 | 6.390 | 2.380 |
Rmerge | 0.046 | 0.027 | 0.420 |
Total number of observations | 132900 | ||
Number of reflections | 19222 | ||
<I/σ(I)> | 16.2 | ||
Completeness [%] | 99.1 | 99.3 | 86.6 |
Redundancy | 6.9 | 6.3 | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 288 | 0.1 M Bis-Tris, pH 6.5, 0.2 M ammonium acetate, 25% PEG 3350 |