4X1W
Crystal structure of unbound RHDVb P domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-09-10 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.984463 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 59.190, 83.130, 118.290 |
Unit cell angles | 90.00, 93.21, 90.00 |
Refinement procedure
Resolution | 19.798 - 1.950 |
R-factor | 0.1814 |
Rwork | 0.180 |
R-free | 0.21240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4egt |
RMSD bond length | 0.005 |
RMSD bond angle | 0.981 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.800 | 2.000 | |
High resolution limit [Å] | 1.950 | 8.720 | 1.950 |
Rmerge | 0.166 | 0.052 | 0.768 |
Rmeas | 0.187 | 0.059 | 0.935 |
Total number of observations | 384589 | ||
Number of reflections | 83210 | 902 | 6082 |
<I/σ(I)> | 7.82 | 23.96 | 1.35 |
Completeness [%] | 99.6 | 90.4 | 98.4 |
Redundancy | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 291 | Lithium chloride, PEG 6000, Citric Acid |