4WWU

Structure of Mex67:Mtr2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04-1
Synchrotron site	Diamond
Beamline	I04-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2014-01-07
Detector	DECTRIS PILATUS 2M
Wavelength(s)	0.9200
Spacegroup name	P 1 21 1
Unit cell lengths	100.610, 76.720, 199.120
Unit cell angles	90.00, 94.09, 90.00

Refinement procedure

Resolution	49.653 - 3.301
R-factor	0.2311
Rwork	0.228
R-free	0.28430
RMSD bond length	0.004
RMSD bond angle	0.813
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	49.700
High resolution limit [Å]	3.300
Number of reflections	44836
<I/σ(I)>	5.1
Completeness [%]	97.4
Redundancy	3.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		291	See publication for details. Precipitant was 10 % PEG 8000, 0.01 M zinc acetate, 0.1 M Tris-HCl pH 8.0.