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4WP4

Hev b 6.02 (hevein) extracted from surgical gloves

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007 HF
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2014-01-27
DetectorRIGAKU RAXIS IV++
Wavelength(s)1.54
Spacegroup nameP 31 2 1
Unit cell lengths37.330, 37.330, 48.777
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution26.947 - 1.430
R-factor0.1529
Rwork0.151
R-free0.16640
Structure solution methodSAD
RMSD bond length0.014
RMSD bond angle1.457
Refinement softwarePHENIX ((phenix.refine: dev_1810))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]26.9501.480
High resolution limit [Å]1.4301.430
Rmerge0.0580.186
Number of reflections13802
<I/σ(I)>64.624.4
Completeness [%]99.096.7
Redundancy11.810.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP5.52910.1M sodium citrate, 2M ammonium sulfate

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