4WOC

Proteinase-K Post-Surface Acoustic Waves

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007
Temperature [K]	100
Detector technology	CCD
Collection date	2014-05-10
Detector	RIGAKU SATURN 944+
Wavelength(s)	1.54
Spacegroup name	P 43 21 2
Unit cell lengths	67.687, 67.687, 102.010
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.737 - 1.601
R-factor	0.1759
Rwork	0.174
R-free	0.20730
RMSD bond length	0.006
RMSD bond angle	1.009
Refinement software	PHENIX

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.600
Number of reflections	31109
<I/σ(I)>	10.9
Completeness [%]	97.0
Redundancy	3.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	298	0.6 - 1.6 Ammonium Sulfate, 0.1 M Tris, pH 8.0