4WO9

Lysozyme Post-Surface Acoustic Waves

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CHESS BEAMLINE A1
Synchrotron site	CHESS
Beamline	A1
Temperature [K]	100
Detector technology	CCD
Collection date	2014-03-30
Detector	ADSC QUANTUM 210
Wavelength(s)	0.978
Spacegroup name	P 43 21 2
Unit cell lengths	79.206, 79.206, 37.644
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.285 - 1.990
R-factor	0.1521
Rwork	0.147
R-free	0.20220
RMSD bond length	0.007
RMSD bond angle	1.090
Refinement software	PHENIX

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.990
Number of reflections	59994
<I/σ(I)>	21.5
Completeness [%]	97.0
Redundancy	7.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	BATCH MODE	4.6	277	1M NaCl, 25% Glycerol, 0.1 M Na Acetate, pH 4.6, gentle agitation