4WM0
Crystal structure of mouse Xyloside xylosyltransferase 1 complexed with acceptor ligand
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X25 |
| Synchrotron site | NSLS |
| Beamline | X25 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-08-15 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.1000 |
| Spacegroup name | P 3 |
| Unit cell lengths | 89.541, 89.541, 42.979 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 77.540 - 2.370 |
| R-factor | 0.18989 |
| Rwork | 0.188 |
| R-free | 0.23283 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.196 |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.450 |
| High resolution limit [Å] | 2.370 | 2.370 |
| Rmerge | 0.061 | 0.196 |
| Number of reflections | 15616 | |
| <I/σ(I)> | 22.6 | 6.5 |
| Completeness [%] | 99.6 | 96 |
| Redundancy | 4.8 | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 0.2 M Li2SO4, 0.1 M Bis-Tris, and 21% PEG3350 |
