4WLI
Stationary Phase Survival Protein YuiC from B.subtilis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-06-30 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.92000 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 50.010, 117.270, 61.000 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.798 - 1.760 |
R-factor | 0.1642 |
Rwork | 0.162 |
R-free | 0.20150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wjt |
RMSD bond length | 0.016 |
RMSD bond angle | 1.495 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.800 | 1.790 |
High resolution limit [Å] | 1.760 | 1.760 |
Rmerge | 0.098 | 0.745 |
Number of reflections | 18150 | |
<I/σ(I)> | 13 | 2.5 |
Completeness [%] | 99.8 | 99.6 |
Redundancy | 7.3 | 7.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289 | 0.2M ammonium chloride, 25 (v/v) glycerol ethoxylate, 0.1M HEPES pH7.5 |