4WIZ
Crystal structure of Grouper nervous necrosis virus-like particle at 3.6A
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL44XU |
| Synchrotron site | SPring-8 |
| Beamline | BL44XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-04-09 |
| Detector | RAYONIX MX225HE |
| Wavelength(s) | 0.90 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 477.355, 422.735, 337.893 |
| Unit cell angles | 90.00, 134.03, 90.00 |
Refinement procedure
| Resolution | 263.910 - 3.600 |
| R-factor | 0.2567 |
| Rwork | 0.255 |
| R-free | 0.29680 |
| Structure solution method | AB INITIO PHASING |
| RMSD bond length | 0.016 |
| RMSD bond angle | 1.767 |
| Data scaling software | HKL-2000 |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 266.000 |
| High resolution limit [Å] | 3.600 |
| Number of reflections | 549703 |
| <I/σ(I)> | 7.2 |
| Completeness [%] | 98.9 |
| Redundancy | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.2 | 291 | 0.2 M Sodium formate, 20% (w/v) PEG 3350, pH7.2 |
