4WAC
Crystal Structure of TarM
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-04-30 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 1.07 |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 124.749, 124.749, 223.255 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.624 - 2.400 |
| R-factor | 0.2173 |
| Rwork | 0.215 |
| R-free | 0.25150 |
| Structure solution method | SAD |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.326 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | SHARP |
| Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 49.000 | 2.460 | |
| High resolution limit [Å] | 2.400 | 10.730 | 2.400 |
| Rmerge | 0.119 | 0.032 | 1.581 |
| Rmeas | 0.126 | 0.034 | 1.672 |
| Total number of observations | 398620 | ||
| Number of reflections | 40713 | 553 | 2909 |
| <I/σ(I)> | 14.79 | 47.53 | 1.69 |
| Completeness [%] | 99.8 | 97 | 98.5 |
| Redundancy | 9.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 289 | imidazole, magnesium acetate, PEG 1000 |
