4W98

Acinetobacter baumannii SDF NDK

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	180
Detector technology	CCD
Collection date	2014-07-12
Detector	ADSC QUANTUM 315
Wavelength(s)	0.979
Spacegroup name	I 2 2 2
Unit cell lengths	61.726, 76.962, 82.239
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.050 - 1.430
R-factor	0.164
Rwork	0.163
R-free	0.18900
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4dut
RMSD bond length	0.006
RMSD bond angle	1.004
Refinement software	PHENIX ((PHENIX.REFINE: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	56.200
High resolution limit [Å]	1.350
Number of reflections	43528
<I/σ(I)>	51
Completeness [%]	99.3
Redundancy	7.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		289	potassium sodium tartrate tetrahydrate, PEG 3350