4W6Q
Glycosyltransferase C from Streptococcus agalactiae
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-ID |
| Synchrotron site | APS |
| Beamline | 22-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2010-04-05 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 1.03317 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 77.204, 99.270, 188.214 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 29.911 - 2.700 |
| R-factor | 0.1866 |
| Rwork | 0.184 |
| R-free | 0.28400 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.390 |
| Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 2.700 |
| Number of reflections | 40273 |
| <I/σ(I)> | 16.241 |
| Completeness [%] | 98.2 |
| Redundancy | 5.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3350, Ammonium Sulfate, Tris, Glycerol |
