4W1O

PDE4D complexed with inhibitor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	OTHER
Temperature [K]	100
Collection date	2007-01-28
Wavelength(s)	1.5418
Spacegroup name	P 21 21 21
Unit cell lengths	99.426, 112.671, 161.077
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	92.450 - 2.200
R-factor	0.23953
Rwork	0.237
R-free	0.28116
RMSD bond length	0.011
RMSD bond angle	1.261
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	92.450
High resolution limit [Å]	2.200
Number of reflections	91831
<I/σ(I)>	9
Completeness [%]	99.5
Redundancy	3.76

Crystallization Conditions

crystal ID	method	pH	temperature	details
1