4V44
E. COLI (lacZ) BETA-GALACTOSIDASE IN COMPLEX WITH 2-F-LACTOSE
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site | Photon Factory |
Beamline | BL-6A |
Temperature [K] | 288 |
Detector technology | IMAGE PLATE |
Collection date | 1994-10-22 |
Detector | RIGAKU |
Wavelength(s) | 1.00 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 107.600, 207.300, 510.300 |
Unit cell angles | 90.00, 95.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.700 |
R-factor | 0.234 |
Rwork | 0.234 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1F49 |
RMSD bond length | 0.015 |
RMSD bond angle | 2.360 |
Data reduction software | WEIS |
Data scaling software | CCP4 |
Phasing software | TNT |
Refinement software | TNT |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.740 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.090 | 0.410 |
Number of reflections | 409961 | |
<I/σ(I)> | 6 | 1.7 |
Completeness [%] | 66.0 | 37.9 |
Redundancy | 1.8 | 1.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.9 | 295 | Cacodylate, PEG 8000, MgSO4, NaCl, BME, pH 5.9, VAPOR DIFFUSION, HANGING DROP at 295K, pH 5.90 |