4V0Q

Dengue Virus Full Length NS5 Complexed with SAH

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS
Synchrotron site	SLS
Beamline	X10SA
Temperature [K]	100
Collection date	2014-02-24
Spacegroup name	P 21 21 2
Unit cell lengths	95.129, 151.445, 69.124
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.184 - 2.300
R-factor	0.1935
Rwork	0.191
R-free	0.24640
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	PDB ENTRIES 3P97 AND 2J7U
RMSD bond length	0.004
RMSD bond angle	0.803
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall
Low resolution limit [Å]	39.180
High resolution limit [Å]	2.300
Rmerge	0.080
Number of reflections	41247
<I/σ(I)>	9.5
Completeness [%]	91.8
Redundancy	3.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1