4UZR
Crystal Structure of Pyrococcus horikoshii Ph1500
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-11-29 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 62.779, 184.169, 172.142 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.988 - 2.652 |
R-factor | 0.2022 |
Rwork | 0.200 |
R-free | 0.25180 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.800 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.100 | 2.810 |
High resolution limit [Å] | 2.650 | 2.650 |
Rmerge | 0.070 | 0.760 |
Number of reflections | 28988 | |
<I/σ(I)> | 14.8 | 2.13 |
Completeness [%] | 98.5 | 97.5 |
Redundancy | 4.38 | 4.46 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 295 | SITTING DROP, 295 K, 30 %(V/V) PEG 400, 200 MM SODIUM CITRATE, 100 MM TRIS PH 8.5 |