4UZI
Crystal Structure of AauDyP Complexed with Imidazole
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID14-4 |
| Synchrotron site | ESRF |
| Beamline | ID14-4 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-10-08 |
| Detector | ADSC QUANTUM 315r |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 67.330, 45.710, 140.470 |
| Unit cell angles | 90.00, 91.61, 90.00 |
Refinement procedure
| Resolution | 47.510 - 2.100 |
| R-factor | 0.18239 |
| Rwork | 0.179 |
| R-free | 0.23867 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4au9 |
| RMSD bond length | 0.004 |
| RMSD bond angle | 0.763 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.500 | 2.220 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.110 | 0.390 |
| Number of reflections | 50456 | |
| <I/σ(I)> | 9.31 | 2.72 |
| Completeness [%] | 99.2 | 95.8 |
| Redundancy | 3.5 | 3.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 8 | 30% MPD, 10% PEG 4000, 100 MM IMIDAZOLE-HCL PH 8.0 |
