4UXM
Crystal Structure of Struthiocalcin-1, a different crystal form.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 100 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 32.670, 55.910, 72.060 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 44.173 - 1.500 |
| R-factor | 0.1894 |
| Rwork | 0.188 |
| R-free | 0.21320 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.017 |
| RMSD bond angle | 1.605 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALE |
| Phasing software | CRANK |
| Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.170 | 44.170 |
| High resolution limit [Å] | 1.500 | 7.570 |
| Rmerge | 0.170 | 0.090 |
| Number of reflections | 21799 | |
| <I/σ(I)> | 11.1 | |
| Completeness [%] | 99.8 | 99.8 |
| Redundancy | 15.4 | 11.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 15 % W/V MPD, 5 % W/V PEG 4000, 100 MM IMIDAZOLE-HCL PH 8.0.(A4JB7) |
