4UX1
Cryo-EM structure of antagonist-bound E2P gastric H,K-ATPase (SCH.E2. AlF)
Experimental procedure
| Temperature [K] | 4 |
| Collection date | 2013-10-29 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 140.900, 111.300, 320.000 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 128.950 - 8.000 |
| R-factor | 0.507 |
| Rwork | 0.507 |
| R-free | 0.51600 |
| RMSD bond length | 0.024 |
| RMSD bond angle | 2.800 |
| Data scaling software | MRC (SUITE) |
| Phasing software | MRC |
| Refinement software | CNS (1.3) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 129.000 |
| High resolution limit [Å] | 8.000 |
| Number of reflections | 35798 |
| Completeness [%] | 52.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.8 | pH 4.8 |
