4UTK

XenA - reduced - Y183F variant

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	BESSY BEAMLINE 14.1
Synchrotron site	BESSY
Beamline	14.1
Temperature [K]	100
Detector technology	CCD
Detector	MARMOSAIC 225 mm CCD
Spacegroup name	I 2 2 2
Unit cell lengths	57.670, 83.450, 157.130
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.835 - 1.440
R-factor	0.1473
Rwork	0.146
R-free	0.17770
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	3l5l
RMSD bond length	0.011
RMSD bond angle	1.219
Refinement software	PHENIX ((PHENIX.REFINE))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	28.840	1.490
High resolution limit [Å]	1.440	1.440
Rmerge	0.060	0.580
Number of reflections	68214
<I/σ(I)>	13.63	2.25
Completeness [%]	99.0	99.54
Redundancy	3.6	3.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1