4US5
Crystal Structure of apo-MsnO8
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2009-02-12 |
| Detector | DECTRIS PILATUS 2M-F |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 85.005, 102.902, 160.697 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 49.050 - 1.800 |
| R-factor | 0.18941 |
| Rwork | 0.188 |
| R-free | 0.21650 |
| Structure solution method | OTHER |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.299 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 49.000 |
| High resolution limit [Å] | 1.800 |
| Rmerge | 0.110 |
| Number of reflections | 130902 |
| Completeness [%] | 100.0 |
| Redundancy | 13.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
