4UO8
Structure of the A_Canine_Colorado_17864_06 H3 haemagglutinin in complex with 6SO4-3SLN
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Detector | DECTRIS PILATUS 2M |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 97.289, 97.289, 348.267 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 48.690 - 3.000 |
| R-factor | 0.20926 |
| Rwork | 0.207 |
| R-free | 0.25084 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4uo4 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.286 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.640 | 3.180 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.100 | 0.590 |
| Number of reflections | 20478 | |
| <I/σ(I)> | 21.9 | 5.1 |
| Completeness [%] | 99.5 | 99.1 |
| Redundancy | 10.6 | 10.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
