4UO4

Structure of the A_Canine_Colorado_17864_06 H3 haemagglutinin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	P 63 2 2
Unit cell lengths	96.405, 96.405, 347.128
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	173.560 - 2.600
R-factor	0.20073
Rwork	0.199
R-free	0.24371
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4uo0
RMSD bond length	0.011
RMSD bond angle	1.655
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	REFMAC (5.8.0069)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.200	2.740
High resolution limit [Å]	2.600	2.600
Rmerge	0.060	0.660
Number of reflections	30387
<I/σ(I)>	17.1	3
Completeness [%]	99.6	99.2
Redundancy	5.2	5.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1