4UNY

Structure of the A_Equine_Newmarket_2_93 H3 haemagglutinin in complex with 6SO4-3SLN

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I02
Synchrotron site	Diamond
Beamline	I02
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 2M
Spacegroup name	P 21 21 21
Unit cell lengths	98.853, 124.873, 163.648
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	99.270 - 2.900
R-factor	0.19383
Rwork	0.191
R-free	0.23743
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4unw
RMSD bond length	0.005
RMSD bond angle	1.197
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0069)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.760	2.980
High resolution limit [Å]	2.900	2.900
Rmerge	0.080	0.660
Number of reflections	45591
<I/σ(I)>	18.9	2.7
Completeness [%]	99.9	100
Redundancy	6.6	6.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1