4UNX

Structure of the A_Equine_Newmarket_2_93 H3 haemagglutinin in complex with 3SLN

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS 6M
Spacegroup name	P 21 21 21
Unit cell lengths	100.485, 102.247, 228.371
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	114.190 - 3.200
R-factor	0.32058
Rwork	0.319
R-free	0.35391
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4unw
RMSD bond length	0.004
RMSD bond angle	0.887
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0069)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	52.240	3.310
High resolution limit [Å]	3.200	3.200
Rmerge	0.150	0.750
Number of reflections	39591
<I/σ(I)>	9.6	2.6
Completeness [%]	100.0	100
Redundancy	7.3	7.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1