4UM8
Crystal structure of alpha V beta 6
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-07-15 |
Detector | MARRESEARCH |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 184.450, 170.010, 102.390 |
Unit cell angles | 90.00, 98.68, 90.00 |
Refinement procedure
Resolution | 48.656 - 2.852 |
R-factor | 0.2395 |
Rwork | 0.238 |
R-free | 0.28080 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4g1m |
RMSD bond length | 0.004 |
RMSD bond angle | 0.718 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.920 |
High resolution limit [Å] | 2.850 | 2.850 |
Rmerge | 0.180 | |
Number of reflections | 69912 | |
<I/σ(I)> | 4.8 | 0.33 |
Completeness [%] | 97.4 | 91 |
Redundancy | 2.4 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | 15% PEG 4000, 0.1 M NACACODYLATE, PH 6.0 |