4UDS

Crystal structure of MbdR regulator from Azoarcus sp. CIB

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Detector	DECTRIS PILATUS3 6M
Spacegroup name	I 2 2 2
Unit cell lengths	47.030, 56.210, 143.820
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	52.350 - 1.760
R-factor	0.1936
Rwork	0.191
R-free	0.24948
Structure solution method	MAD
Starting model (for MR)	NONE
RMSD bond length	0.023
RMSD bond angle	1.818
Refinement software	REFMAC (5.6.0111)

Data quality characteristics

	Overall
Low resolution limit [Å]	52.350
High resolution limit [Å]	1.760
Rmerge	0.070
Number of reflections	17349
Completeness [%]	95.7
Redundancy	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1