4U77

BTB domain from Drosophila CP190

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE BM30A
Synchrotron site	ESRF
Beamline	BM30A
Temperature [K]	100
Detector technology	CCD
Collection date	2012-06-13
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.07230
Spacegroup name	P 32 2 1
Unit cell lengths	84.979, 84.979, 40.870
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	36.797 - 2.030
R-factor	0.1937
Rwork	0.191
R-free	0.24140
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.037
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.8.4_1496))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.490	2.140
High resolution limit [Å]	2.030	2.030
Rmerge		0.516
Number of reflections	11252
<I/σ(I)>	16.6
Completeness [%]	100.0	100
Redundancy	6.9	7.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION	7.5	291	Na/K PO4 1.6 M, HEPES 0.1 M