4U6Z
HsMetAP(F309M) in complex with 1-amino-2-propylpentyl)phosphonic acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-03-24 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.137, 77.331, 47.153 |
Unit cell angles | 90.00, 93.08, 90.00 |
Refinement procedure
Resolution | 18.810 - 1.800 |
R-factor | 0.169 |
Rwork | 0.167 |
R-free | 0.20400 |
RMSD bond length | 0.021 |
RMSD bond angle | 1.939 |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 19.000 |
High resolution limit [Å] | 1.800 |
Number of reflections | 30443 |
<I/σ(I)> | 3.5 |
Completeness [%] | 97.1 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 15% PEG-MME, 100mM HEPES, PH 6 |