4U3Y
Apo Mitogen-activated protein kinase kinase kinase kinase 4 (MAP4K4)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-10-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 80.407, 80.839, 92.953 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.930 - 1.450 |
R-factor | 0.1838 |
Rwork | 0.183 |
R-free | 0.20690 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.010 |
RMSD bond angle | 1.030 |
Data scaling software | SCALEPACK |
Refinement software | BUSTER (2.11.4) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 1.500 |
High resolution limit [Å] | 1.450 | 3.120 | 1.450 |
Rmerge | 0.062 | 0.029 | 0.741 |
Total number of observations | 779291 | ||
Number of reflections | 108043 | ||
<I/σ(I)> | 12.7 | ||
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 7.2 | 7.3 | 7.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.3 | 292 | 0.2 M potassium citrate, pH 8.3, 20% PEG 3350 |