4U3H

Crystal structure of FN3con

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron site	Australian Synchrotron
Beamline	MX1
Temperature [K]	100
Detector technology	CCD
Collection date	2013-12-04
Detector	ADSC QUANTUM 210r
Wavelength(s)	0.9537
Spacegroup name	P 41 3 2
Unit cell lengths	86.100, 86.100, 86.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	35.150 - 1.980
R-factor	0.1992
Rwork	0.197
R-free	0.24320
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2ck2
RMSD bond length	0.013
RMSD bond angle	1.366
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	35.150	2.030
High resolution limit [Å]	1.980	1.980
Rmerge	0.108	0.792
Number of reflections	8078
<I/σ(I)>	28.5	5.8
Completeness [%]	100.0	100
Redundancy	2	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	4.2	288	0.1M phosphate-citrate pH 4.2 and 40% PEG 300