4U1Y

Full length GluA2-FW-(R,R)-2b complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 5.0.2
Synchrotron site	ALS
Beamline	5.0.2
Temperature [K]	100
Detector technology	CCD
Collection date	2013-01-12
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	105.250, 151.440, 330.490
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.973 - 3.900
R-factor	0.27
Rwork	0.268
R-free	0.30350
RMSD bond length	0.005
RMSD bond angle	1.021
Data reduction software	XDS
Data scaling software	Aimless
Refinement software	PHENIX (1.8.2_1309)

Data quality characteristics

	Overall
Low resolution limit [Å]	64.990
High resolution limit [Å]	3.700
Number of reflections	56784
<I/σ(I)>	6.93
Completeness [%]	99.1
Redundancy	4.12

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	0.1 M imidazole pH 6.2, 9% PEG1450, 3% TMAO