4TUN
Crystal structure of Chicken egg white lysozyme adduct with Organophosphorus pesticide Monochrotophos
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | BRUKER AXS MICROSTAR |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2012-07-23 |
| Detector | MAR scanner 345 mm plate |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 43 |
| Unit cell lengths | 78.720, 78.720, 37.020 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 35.200 - 1.925 |
| R-factor | 0.17465 |
| Rwork | 0.172 |
| R-free | 0.22908 |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.857 |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 78.700 |
| High resolution limit [Å] | 1.925 |
| Number of reflections | 15434 |
| <I/σ(I)> | 4 |
| Completeness [%] | 90.1 |
| Redundancy | 3.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 289 | Sodium Acetate, Sodium Chloride |
