4TUM
Crystal structure of Ankyrin Repeat Domain of AKR2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 5C (4A) |
| Synchrotron site | PAL/PLS |
| Beamline | 5C (4A) |
| Temperature [K] | 103 |
| Detector technology | CCD |
| Collection date | 2010-06-23 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 68.331, 59.381, 84.860 |
| Unit cell angles | 90.00, 107.33, 90.00 |
Refinement procedure
| Resolution | 19.977 - 2.300 |
| R-factor | 0.2074 |
| Rwork | 0.206 |
| R-free | 0.22410 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.398 |
| Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.300 |
| Number of reflections | 33241 |
| <I/σ(I)> | 27.4 |
| Completeness [%] | 98.7 |
| Redundancy | 4.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | PEG |
