4TTD
Structure of a lysozyme antibody complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-02-06 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.979 |
| Spacegroup name | P 1 |
| Unit cell lengths | 63.900, 64.300, 76.600 |
| Unit cell angles | 102.40, 101.80, 102.40 |
Refinement procedure
| Resolution | 41.220 - 2.150 |
| R-factor | 0.2561 |
| Rwork | 0.255 |
| R-free | 0.27890 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.050 |
| Refinement software | BUSTER (2.11.5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.410 | 2.230 |
| High resolution limit [Å] | 2.150 | 2.150 |
| Rmerge | 0.338 | |
| Number of reflections | 57649 | |
| <I/σ(I)> | 6.4 | 1.5 |
| Completeness [%] | 94.4 | 95 |
| Redundancy | 1.64 | 1.64 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 100mM PCTP pH 4.5, 25% w/v Peg3350, ethanol 5% |
