4TS1

CRYSTAL STRUCTURE OF A DELETION MUTANT OF A TYROSYL-T/RNA SYNTHETASE COMPLEXED WITH TYROSINE

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	95.460, 67.060, 61.370
Unit cell angles	90.00, 90.78, 90.00

Refinement procedure

Resolution	8.000 * - 2.500
R-factor	0.187
RMSD bond length	0.017
RMSD bond angle	0.044
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.500 *
Rmerge	0.058 *
Total number of observations	64683 *
Number of reflections	26176 *
Completeness [%]	94.3 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	15 (mM)
2	1	drop	tyrosine	1 (mM)
3	1	drop	polyethylene glycol 4000	6 (%(w/v))
4	1	reservoir	polyethylene glycol	12 (%)