4TLL

Crystal structure of GluN1/GluN2B NMDA receptor, structure 1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALS BEAMLINE 8.2.1
Synchrotron site	ALS
Beamline	8.2.1
Temperature [K]	100
Detector technology	CCD
Collection date	2014-04-20
Detector	ADSC QUANTUM 315r
Wavelength(s)	1.0
Spacegroup name	C 1 2 1
Unit cell lengths	201.460, 117.260, 218.760
Unit cell angles	90.00, 106.70, 90.00

Refinement procedure

Resolution	48.080 - 3.590
R-factor	0.2684
Rwork	0.266
R-free	0.30500
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.878
Refinement software	PHENIX ((phenix.refine: 1.9_1692))

Data quality characteristics

	Overall
Low resolution limit [Å]	48.100
High resolution limit [Å]	3.470
Number of reflections	54471
<I/σ(I)>	6.44
Completeness [%]	85.7
Redundancy	6.51

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	Vapor diffusion, hanging drop, temperature 293K