4TGL

CATALYSIS AT THE INTERFACE: THE ANATOMY OF A CONFORMATIONAL CHANGE IN A TRIGLYCERIDE LIPASE

Experimental procedure

Spacegroup name	C 2 2 21
Unit cell lengths	48.300, 93.900, 122.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 * - 2.650 *
R-factor	0.129
RMSD bond length	0.019
RMSD bond angle	0.069
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	4.820 *
High resolution limit [Å]	2.650 *
Rmerge	0.102 *
Number of reflections	6017 *
Completeness [%]	74.0 *
Redundancy	3.6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	PEG600	8-12 (%)
2	1	drop	protein	20 (mg/mL)