4S1K
Structure of Uranotaenia sapphirina cypovirus (CPV17) polyhedrin at 100 K
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I24 |
| Synchrotron site | Diamond |
| Beamline | I24 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-02-19 |
| Detector | PSI PILATUS 6M |
| Wavelength(s) | 0.9686 |
| Spacegroup name | I 2 3 |
| Unit cell lengths | 104.879, 104.879, 104.879 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 74.000 - 2.200 |
| R-factor | 0.15054 |
| Rwork | 0.148 |
| R-free | 0.19892 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.675 |
| Data reduction software | DIALS |
| Data scaling software | DIALS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 74.000 | 74.160 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Number of reflections | 9376 | |
| Completeness [%] | 99.8 | 99.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | In vivo | 7.5 | 301 | CRYSTALS FORMED NATURALLY WITHIN THE CYTOPLASM AND WERE PURIFIED FROM CELLS, pH 7.5, In vivo, temperature 301K |
