4S0R
Structure of GS-TnrA complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 8.3.1 |
| Synchrotron site | ALS |
| Beamline | 8.3.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-03-04 |
| Detector | ADSC QUANTUM 315r |
| Spacegroup name | P 3 |
| Unit cell lengths | 295.800, 295.800, 103.600 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 147.900 - 3.500 |
| R-factor | 0.243 |
| Rwork | 0.243 |
| R-free | 0.28400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 147.900 |
| High resolution limit [Å] | 3.500 |
| Number of reflections | 118362 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 6.5 | 298 | 25% PEG 400, MES, pH 6.5, 5% PEG 8000, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
