4RLB
Crystal structure of Acinetobacter baumannii CarO2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-02-23 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97949 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 139.602, 139.602, 138.759 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 60.000 - 2.700 |
| R-factor | 0.19203 |
| Rwork | 0.190 |
| R-free | 0.22823 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.796 |
| Data reduction software | XDS |
| Data scaling software | XDS (/ XSCALE) |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 120.899 | 2.830 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Number of reflections | 22490 | |
| Completeness [%] | 99.9 | 100 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 292 | 63% MPD, 0.1 M Tris, pH 8.0, VAPOR DIFFUSION, HANGING DROP, temperature 292K |
