4RL9
Crystal structure of Acinetobacter baumannii CarO1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I04 |
| Synchrotron site | Diamond |
| Beamline | I04 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-07-10 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.9795 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 145.774, 63.260, 73.668 |
| Unit cell angles | 90.00, 119.70, 90.00 |
Refinement procedure
| Resolution | 63.990 - 2.700 |
| R-factor | 0.23497 |
| Rwork | 0.233 |
| R-free | 0.27806 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.586 |
| Data reduction software | XDS |
| Data scaling software | XDS (/ XSCALE) |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 63.990 | 2.830 |
| High resolution limit [Å] | 2.700 | 2.700 |
| Number of reflections | 16167 | |
| Completeness [%] | 99.7 | 99.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 292 | 9% PEG8000, 0.04 M zinc acetate, 0.05 M ADA, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 292K |
