4RL7
Crystal structure of Human galectin-3 CRD in complex with lactose (pH 7.5, PEG6000)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 297 |
| Wavelength(s) | 0.7107 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 36.200, 57.800, 63.000 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 23.763 - 2.000 |
| R-factor | 0.1735 |
| Rwork | 0.166 |
| R-free | 0.24480 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4r9d |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.261 |
| Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 27.583 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 8861 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 7.5 | 297 | pH 7.5, temperature 297K |
