4RB0
Crystal structure of Magnetospirillum gryphiswaldense MSR-1 SeMet-Apo-Fur
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-5A |
| Synchrotron site | Photon Factory |
| Beamline | BL-5A |
| Temperature [K] | 130 |
| Detector technology | CCD |
| Collection date | 2011-05-20 |
| Detector | ADSC QUANTUM 270 |
| Wavelength(s) | 0.97931, 0.9795, 1.000 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 69.156, 78.549, 66.084 |
| Unit cell angles | 90.00, 108.94, 90.00 |
Refinement procedure
| Resolution | 50.000 - 1.850 |
| R-factor | 0.17606 |
| Rwork | 0.174 |
| R-free | 0.20735 |
| Structure solution method | MAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.467 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SHARP |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.780 |
| High resolution limit [Å] | 1.750 | 1.750 |
| Number of reflections | 29381 | |
| Completeness [%] | 85.9 | 17.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 277 | pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K |
